论文标题
在Al-Mn合金中恢复和重结晶期间分散剂对(sub)晶粒的方向取决于(sub)晶粒
Orientation dependent pinning of (sub)grains by dispersoids during recovery and recrystallization in an Al-Mn alloy
论文作者
论文摘要
在热力学处理过程中,可以通过微化学状态控制合金中的晶粒尺寸和纹理。同时降水对恢复和重结晶的影响在这里通过直接将P,CubEnd或Cube取向的(子)晶粒与第二相颗粒(在冷滚动和非等热的AL-MN合金中)直接相关。重结晶状态由粗糙的细长晶粒具有强大的P,较弱的肘,甚至较弱的立方体质地。相关数据可实现取决于对大型组成粒子周围变形区的子边界和亚细胞的分散体密度和大小的定量定量。得出并使用了从子限内分散体中的史密斯 - 安排阻力的新的修改表达式。结果表明,分散体的(子)晶界的阻力取决于方向,并且立方体亚晶粒在恢复和部分重结晶后经历最高的阻力。由于阻力增加而无法实现AL合金中立方体亚晶粒的大小优势,从而促进了粒子刺激的成核(PSN)。在大颗粒周围的变形区中,相对较少和较大的分散体在PSN核上减少了史密斯 - 安排的阻力,从而进一步增强了PSN的效果。与Cubend纹理相比,证实P纹理更强的P纹理的观察结果是P亚晶粒的频率更高,并且这些亚晶粒的生长更快。应用的方法可以更好地理解恢复和重结晶期间方向依赖性成核和生长行为背后的机制,并在Al-MN合金中具有强大的并发降水。特别是,与立方体质地相比,该方法对强P和肘纹理提供了新的见解。
The recrystallized grain size and texture in alloys can be controlled via the microchemistry state during thermomechanical processing. The influence of concurrent precipitation on recovery and recrystallization is here analyzed by directly correlating (sub)grains of P, CubeND or Cube orientation with second-phase particles in a cold-rolled and non-isothermally annealed Al-Mn alloy. The recrystallized state is dominated by coarse elongated grains with a strong P, weaker CubeND and even weaker Cube texture. The correlated data enables orientation dependent quantification of the density and size of dispersoids on sub-boundaries and subgrains in the deformation zones around large constituent particles. A new modified expression for the Smith-Zener drag from dispersoids on sub-boundaries is derived and used. The results show that the drag on (sub)grain boundaries from dispersoids is orientation dependent, with Cube subgrains experiencing the highest drag after recovery and partial recrystallization. The often observed size advantage of Cube subgrains in Al alloys is not realized due to the increased drag, thereby promoting particle-stimulated nucleation (PSN). Relatively fewer and larger dispersoids in deformation zones around large particles give a reduced Smith-Zener drag on PSN nuclei, thus further strengthening the effect of PSN. Observations substantiating the stronger P texture compared to the CubeND texture are a higher frequency of P subgrains and a faster growth of these subgrains. The applied methodology enables a better understanding of the mechanisms behind the orientation dependent nucleation and growth behavior during recovery and recrystallization with strong concurrent precipitation in Al-Mn alloys. In particular, the methodology gives new insights into the strong P and CubeND textures compared to the Cube texture.