论文标题
开发自动化毫米流体平台和快速电化学腐蚀测量的数据分析管道：Zn-Ni的pH研究
Development of an automated millifluidic platform and data-analysis pipeline for rapid electrochemical corrosion measurements: a pH study on Zn-Ni
论文作者
论文摘要
我们描述了基于毫米的扫描液滴单元平台的开发，以快速和自动化的腐蚀。该系统允许在平面样品的局部截面上测量腐蚀特性（例如，通过TAFEL和线性极化电阻测量和线性极化电阻测量以及环状伏安图）的测量。我们的系统是高度自动化和灵活的，可以在样品上进行脚本更改和混合解决方案和点对点运动。我们还创建了一个自动数据分析管道。在这里，我们通过腐蚀一盘电镀Zn $ _ {85} $ ni $ _ {15} $合金在一系列pH值的范围内证明了此工具，并将我们的结果与XPS测量和文献相关联。
We describe the development of a millifluidic based scanning droplet cell platform for rapid and automated corrosion. This system allows for measurement of corrosion properties (e.g., open circuit potential, corrosion current through Tafel and linear polarization resistance measurements, and cyclic voltammograms) on a localized section of a planar sample. Our system is highly automated and flexible, allowing for scripted changing and mixing of solutions and point-to-point motion on the sample. We have also created an automated data analysis pipeline. Here we demonstrate this tool by corroding a plate of electroplated Zn$_{85}$Ni$_{15}$ alloy over a range of pH values and correlate our results with XPS measurements and literature.
