论文标题

高压诱导的AL7075合金中的降水

High pressure induced precipitation in Al7075 alloy

论文作者

Parakh, Abhinav, Lee, Andrew C., Chariton, Stella, Wang, Melody M., Kiani, Mehrdad T., Prakapenka, Vitali B., Gu, X. Wendy

论文摘要

沉淀 - 基质相互作用控制沉淀增强基于Al的合金的机械行为。这些合金发现,由于其低成本和高强度与重量比,从航空航天到汽车和海军行业的广泛应用。由基于Al的合金制成的结构会经历复杂的负载条件,例如高应变率影响,涉及高压。在这里,我们使用钻石砧细胞研究基于Al的AL7075合金在准静态和非静态压力下的行为,高达约53 GPa。原位X射线衍射(XRD)以及压缩前和后压缩透射电子显微镜(TEM)成像用于分析显微结构变化并估计高压强度。我们发现使用准静态压力XRD测量值的散装模量为75.2 +-1.9 GPA。 XRD表明,非静态压力会导致缺陷密度显着增加,并随着压力循环的峰值扩大。 XRD在非静态压力下的XRD映射表明,局部压力最高的区域的缺陷成核的增加最大,而局部压力梯度最大的区域进行了纹理,并且晶粒较大。 TEM分析表明,压力循环导致了许多沉淀物的成核和生长。缺陷和沉淀密度的显着增加会导致高压下AL7075合金的强度增加。

Precipitate-matrix interactions govern the mechanical behavior of precipitate strengthened Al-based alloys. These alloys find a wide range of applications ranging from aerospace to automobile and naval industries due to their low cost and high strength to weight ratio. Structures made from Al-based alloys undergo complex loading conditions such as high strain rate impact, which involves high pressures. Here we use diamond anvil cells to study the behavior of Al-based Al7075 alloy under quasi-hydrostatic and non-hydrostatic pressure up to ~53 GPa. In situ X-ray diffraction (XRD) and pre- and post-compression transmission electron microscopy (TEM) imaging are used to analyze microstructural changes and estimate high pressure strength. We find a bulk modulus of 75.2 +- 1.9 GPa using quasi-hydrostatic pressure XRD measurements. XRD showed that non-hydrostatic pressure leads to a significant increase in defect density and peak broadening with pressure cycling. XRD mapping under non-hydrostatic pressure revealed that the region with the highest local pressure had the greatest increase in defect nucleation, whereas the region with the largest local pressure gradient underwent texturing and had larger grains. TEM analysis showed that pressure cycling led to the nucleation and growth of many precipitates. The significant increase in defect and precipitate density leads to an increase in strength for Al7075 alloy at high pressures.

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