论文标题

紧凑的小角度中子散射仪器的设计研究

A Design Study of a Compact Small-Angle Neutron Scattering Instrument

论文作者

Bleuel, Markus, Siebenbürger, Miriam, Böni, Peter, Schneider, Gerald J.

论文摘要

纳米级结构的确定属于材料科学中的关键任务之一。小角度中子散射(SANS)是研究纳米结构的高度有价值的工具。在这里,我们探讨了要安装在单个基于加速器的脉冲低通量源的紧凑型SAN仪器的可能性,并讨论了结构表征,教育和培训中的应用。对现实设置的蒙特卡洛模拟证明了这种仪器的可行性,理想的测量大约需要7个小时。预期的长度尺度测量范围为0.5 nm至50 nm。简约的设计导致易于操作,低维护仪器,而与大型设施的时间表无关。尺寸,成本和维护与实验室小角度X射线散射(SAXS)仪器相媲美,这使大学的个别研究团队负担得起,并为教育和培训提供了独特的机会。拟议的设置创造了机会,以衡量现有SANS仪器成本的一小部分来衡量超速结构变化,因此可以每周或每月重复率。该概念可以扩展到整个仪器套件,包括广角中子散射(WAN)和衍射,中子反射测量法(NR),中子X射线照相术,光栅干涉法(GI)和及时的伽玛激活分析(PGAA)。

Nanoscale structure determination belongs to one of the crucial tasks in materials science. Small-angle neutron scattering (SANS) is a highly valuable tool to investigate nanostructures. Here, we explore the possibility of a compact SANS instrument to be installed at an individual accelerator based pulsed low-flux source, and discuss applications in structural characterization, education, and training. Monte Carlo simulations of a realistic setup demonstrate the feasibility of such an instrument, with an ideal measurement taking about 7 hours. The anticipated length-scale measurement range is 0.5 nm to 50 nm. The minimalistic design results in an easy to operate, low maintenance instrument, independent of the schedules of large-scale facilities. Size, cost, and maintenance are comparable to laboratory small-angle X-ray scattering (SAXS) instruments, which makes SANS affordable for individual research teams at universities and provides unique chances for education and training. The proposed setup creates the opportunity to measure ultraslow structural changes, at a fraction of the cost of existing SANS instruments, hence enables weekly or monthly repetition rates. The concept can be expanded to an entire suite of instruments, including wide-angle neutron scattering (WANS) and diffraction, neutron reflectometry (NR), neutron radiography, grating interferometry (GI), and prompt gamma activation analysis (PGAA).

扫码加入交流群

加入微信交流群

微信交流群二维码

扫码加入学术交流群,获取更多资源